1. 鎳-鎢-鈷合(he)金電刷鍍液的(de)性質


  鎳-鎢-鈷合金電刷鍍液是在鎳-鎢合金鍍液的基礎上加入少量的硫酸鈷等成分組成的鎳-鎢-鈷鍍液。它是酸性鍍液,pH=1.2~2.4,深綠色,20℃時相對密度為1.29,電導率為2.052 Ω-1·cm-1



2. 鎳-鎢(wu)-鈷合金電刷鍍層的性(xing)質和(he)用途


  鎳-鎢-鈷鍍(du)(du)層(ceng)硬度高,致密、孔隙少(shao),在較高的(de)(de)溫度下仍具(ju)有一定的(de)(de)硬度,其優(you)點(dian)是鍍(du)(du)層(ceng)的(de)(de)應力(li)小,可(ke)沉積較厚(hou)的(de)(de)鍍(du)(du)層(ceng),即可(ke)達(da)0.20mm,主要用來沉積耐磨的(de)(de)表(biao)面層(ceng)。



3. 鎳-鎢-鈷合金電刷鍍液的成分


 硫酸鎳(NiSO4·7H2O)   393g/L  、 硫酸鎂(MgSO4·7H2O)  2g/L


 鎢酸鈉(Na2WO4·2H2O)   23g/L  、冰醋酸(CH3COOH)  20mL/L


 甲酸(HCOOH)  35g/L  、 硼酸(H3BO3) 31mL/L  、氟化鈉(NaF) 5g/L


 檸檬酸(H3C6H5O7·H2O)  42g/L  、硫酸鈉(Na2SO4)  6.5g/L


 十二烷基硫酸鈉[CH3(CH2)11 SO4Na]  0.01~0.001g/L


 硫酸鈷(CoSO4·7H2O)  2g/L   、 硫酸錳(MnSO4·4H2O)  2g/L



4. 鎳-鎢(wu)-鈷(gu)合金(jin)電(dian)刷鍍液的配(pei)制


  在1000mL燒杯(bei)中(zhong)加(jia)(jia)(jia)(jia)入蒸餾(liu)(liu)(liu)水(shui)(shui)(shui)350mL,加(jia)(jia)(jia)(jia)熱(re)至(zhi)(zhi)70℃,加(jia)(jia)(jia)(jia)入硫酸(suan)(suan)(suan)鎳(nie)(nie)393g,攪(jiao)拌(ban)(ban)(ban)溶(rong)(rong)(rong)(rong)(rong)解(jie)(jie)。另(ling)取(qu)250ml,燒杯(bei),加(jia)(jia)(jia)(jia)水(shui)(shui)(shui)100ml,加(jia)(jia)(jia)(jia)熱(re)至(zhi)(zhi)70℃,加(jia)(jia)(jia)(jia)入檸(ning)檬酸(suan)(suan)(suan)42g,攪(jiao)排溶(rong)(rong)(rong)(rong)(rong)解(jie)(jie)后(hou),加(jia)(jia)(jia)(jia)入鴨酸(suan)(suan)(suan)鈉(na)23,加(jia)(jia)(jia)(jia)熱(re)攪(jiao)拌(ban)(ban)(ban)館(guan)解(jie)(jie)后(hou),加(jia)(jia)(jia)(jia)入含(han)硫酸(suan)(suan)(suan)鎳(nie)(nie)的溶(rong)(rong)(rong)(rong)(rong)液(ye)中(zhong),攪(jiao)拌(ban)(ban)(ban)均(jun)(jun)勻。另(ling)取(qu)在250mL燒杯(bei)中(zhong)加(jia)(jia)(jia)(jia)入蒸餾(liu)(liu)(liu)水(shui)(shui)(shui)100ml,加(jia)(jia)(jia)(jia)熱(re)至(zhi)(zhi)70℃,加(jia)(jia)(jia)(jia)入硼(peng)酸(suan)(suan)(suan)31g,加(jia)(jia)(jia)(jia)熱(re)攪(jiao)拌(ban)(ban)(ban)溶(rong)(rong)(rong)(rong)(rong)解(jie)(jie)后(hou),加(jia)(jia)(jia)(jia)入含(han)硫酸(suan)(suan)(suan)鎳(nie)(nie)的溶(rong)(rong)(rong)(rong)(rong)液(ye)中(zhong),攪(jiao)拌(ban)(ban)(ban)均(jun)(jun)勻。另(ling)取(qu)在250mL燒杯(bei)中(zhong)加(jia)(jia)(jia)(jia)蒸餾(liu)(liu)(liu)水(shui)(shui)(shui)50ml,加(jia)(jia)(jia)(jia)熱(re)至(zhi)(zhi)70℃,加(jia)(jia)(jia)(jia)入硫酸(suan)(suan)(suan)鈉(na)6.5g、硫酸(suan)(suan)(suan)鈷2g、硫酸(suan)(suan)(suan)錳28、硫酸(suan)(suan)(suan)鎂2g和(he)氟化(hua)鈉(na)5g,加(jia)(jia)(jia)(jia)熱(re)攪(jiao)拌(ban)(ban)(ban)溶(rong)(rong)(rong)(rong)(rong)解(jie)(jie)后(hou),加(jia)(jia)(jia)(jia)人(ren)含(han)硫酸(suan)(suan)(suan)鎳(nie)(nie)的溶(rong)(rong)(rong)(rong)(rong)液(ye)中(zhong),攪(jiao)拌(ban)(ban)(ban)均(jun)(jun)勻。另(ling)加(jia)(jia)(jia)(jia)十二(er)烷基硫酸(suan)(suan)(suan)鈉(na)0.01~0.001g充分攪(jiao)拌(ban)(ban)(ban)溶(rong)(rong)(rong)(rong)(rong)解(jie)(jie)。再加(jia)(jia)(jia)(jia)人(ren)甲酸(suan)(suan)(suan)35mL 和(he)冰醋(cu)酸(suan)(suan)(suan)20mL,加(jia)(jia)(jia)(jia)熱(re)充分攪(jiao)拌(ban)(ban)(ban)至(zhi)(zhi)溶(rong)(rong)(rong)(rong)(rong)液(ye)透(tou)明。冷(leng)卻至(zhi)(zhi)室溫,用10%稀(xi)(xi)硫酸(suan)(suan)(suan)或稀(xi)(xi)氫氧化(hua)鈉(na)溶(rong)(rong)(rong)(rong)(rong)液(ye)調節溶(rong)(rong)(rong)(rong)(rong)液(ye)pH為2.將溶(rong)(rong)(rong)(rong)(rong)液(ye)倒入1000mL量(liang)(liang)筒或量(liang)(liang)瓶中(zhong),加(jia)(jia)(jia)(jia)蒸餾(liu)(liu)(liu)水(shui)(shui)(shui)至(zhi)(zhi)刻度。



5. 鎳(nie)-鎢-鈷合(he)金鍍液工藝規范


 鎳-鎢-鈷合金鍍(du)液(ye)性能上比(bi)較類(lei)似于鎳-鎢合金鍍(du)液(ye)。


 耗電系(xi)數:0.21A·h/(d㎡·μm);


 工作電壓:6~12V(最佳(jia)10~12V);


 陰陽極相(xiang)對運動(dong)速率:6~12m/min;


 工作溫度(du):30~50℃.


 循(xun)環(huan)使用(yong)過(guo)程(cheng)可參照(zhao)鎳-鎢合金刷鍍液(ye)。