1. 堿(jian)性銅電刷(shua)鍍液的性質
堿(jian)性(xing)銅電刷鍍液呈微堿(jian)性(xing),pH為7~8,顯藍紫(zi)色(se)。銅離子(zi)含量均為50g/L,20℃時相對密度(du)為1.13,電導率為0.142 Ω-1·cm-1。工作通風(feng)要(yao)好,不要(yao)用手(shou)接觸鍍液。
2. 堿性銅(tong)電刷鍍新的性質及(ji)用途
堿(jian)性銅(tong)電(dian)(dian)刷(shua)鍍銅(tong)層結晶(jing)致密,結合力(li)好多用作過渡層或中間層、釬焊層和導電(dian)(dian)層,防(fang)滲碳和防(fang)氮化層。
3. 堿性銅電(dian)刷鍍(du)液成分,見表4-46.
4. 堿性銅電刷(shua)鍍(du)液(ye)的配制(zhi)
以(yi)配方3為例(li),在(zai)1000mL燒杯中加(jia)(jia)(jia)入(ru)硫(liu)(liu)酸(suan)銅(tong)(tong)250g,蒸(zheng)餾水250mL,加(jia)(jia)(jia)熱(re)攪(jiao)拌(ban)溶(rong)解,冷(leng)卻至20℃,量(liang)(liang)取二乙胺250mL,在(zai)攪(jiao)拌(ban)下緩慢滴(di)入(ru)硫(liu)(liu)酸(suan)銅(tong)(tong)溶(rong)液(ye),由于(yu)是(shi)放熱(re)反應,溫度升高后要冷(leng)卻后再加(jia)(jia)(jia)。在(zai)500mL的燒杯中,加(jia)(jia)(jia)入(ru)氨三乙酸(suan)150g,加(jia)(jia)(jia)蒸(zheng)餾水100mL,加(jia)(jia)(jia)入(ru)氫(qing)氧(yang)化(hua)鈉92g,攪(jiao)拌(ban)使(shi)兩者溶(rong)解,冷(leng)卻后加(jia)(jia)(jia)入(ru)硝酸(suan)銨50g,硫(liu)(liu)酸(suan)鈉20g,攪(jiao)拌(ban)溶(rong)解后加(jia)(jia)(jia)入(ru)硫(liu)(liu)酸(suan)銅(tong)(tong)乙二胺溶(rong)液(ye)中,冷(leng)卻后加(jia)(jia)(jia)入(ru)1000mL量(liang)(liang)筒或(huo)量(liang)(liang)瓶中,加(jia)(jia)(jia)蒸(zheng)餾水稀(xi)釋至刻度,最后測量(liang)(liang)pH,低(di)(di)了,加(jia)(jia)(jia)少許10%氫(qing)氧(yang)化(hua)鈉溶(rong)液(ye)以(yi)便(bian)升高pH;高了,加(jia)(jia)(jia)少許10%硫(liu)(liu)酸(suan)溶(rong)液(ye)以(yi)便(bian)降低(di)(di)pH。
5. 操作方法及(ji)工藝規(gui)范(fan)
耗電系數:0.18A·h/(d㎡2·μm),在循環使用過程中耗電系數不變(bian);
工作電壓:6~15V;
接電(dian)方式:按正(zheng)(zheng)極(ji)(ji)性(xing)連接,工(gong)件接負極(ji)(ji),鍍(du)筆(bi)接正(zheng)(zheng)極(ji)(ji);
陰陽極相對運(yun)動速率:10~30m/min;
使用溫度:20~50℃;
在循環使用過程中(zhong),銅(tong)離子濃(nong)度在剩余溶液(ye)(ye)中(zhong)增加,堿銅(tong)刷鍍(du)液(ye)(ye)屬富集鍍(du)液(ye)(ye)。
沉積速率(lv):12.8μm/min;
鍍層最大厚度:一般為0.02~0.03mm.